A When using a
glove box for chemical synthesis experiments, the safety operating procedures that need to be followed include preliminary preparation:
1. Check the appearance of the glove box,
gloves, and
gas purification system for normal operation, prepare experimental materials, and perform pre-treatment;
2. Parameter setting: Set the parameters of the glove box according to the operation manual requirements to ensure that the purity of the inert gas meets the standard;
3. Experimental procedure: Conduct the experiment gently and slowly using gloves in the glove box, following the experimental steps;
4. Environmental monitoring: Continuously monitor the environmental parameters inside the glove box, such as temperature, humidity, water oxygen content, etc;
5. End of experiment: Clean up waste and remaining materials, turn off experimental equipment and instruments, keep the glove box circulation system open, and lay a foundation for the next experiment in advance.
6. Regular maintenance: check the sealing performance, operation status of the gas circulation system, clean components such as filters and pipelines, regularly replace gloves, receive professional training, etc.